Chemistry 193- Chemical Instrumentation

1. Text and Laboratory Manual:

  1. Microcomputer and Electronic Instrumentation: Making the Right Connection, a 464-page textbook by H.V. Malmstadt, C. G. Enke, and S.R. Crouch published by the American Chemical Society, Washington, DC, 1994.
  2. Experiment Manual: Laboratory Electronics for Scientists Hand On by H.V. Malmstadt, C. G. Enke, and S.R. Crouch published by the American Chemical Society, Washington , DC , 2nd Ed., 1994.

Call GWU Bookstore for Availability: 202-994-1439, 6873

2. Level:

Graduate and senior undergraduate students in any area of science may register. No electronics experience is necessary.

3. Class Schedule:

The hours are:
Lectures on M at 9-10:50 AM, Sam 311
Laboratory on W at 9:00-11:50 AM, Cor 406

4. Exams:

  1. Midterm (33.33%); first Monday, month of October
  2. Final (33.33%)
  3. Project and Active Participation in Class (33.33%); Computer Interfacing and Programming project due one week after the end of classes.

5. Office Hours:

Tuesday & Thursday 2 ‑ 3 PM or by appointment.  For appointment, please call 202‑994‑6480, or see me in Samson 211 (Office) or Cor-310 & 309 (Research Laboratories), or send an Email to montaser@gwu.edu .

6. Expectations:

  1. Be on time and read and re-read a minimum of one chapter/week.
  2. If you do not come to any exams due to an illness, you must bring a note from your physician.
  3. To get an A grade in this course, you must: 1) read the relevant chapters before coming to class; 2) take good notes during the lectures; 3) read the related chapter right after the lecture; and 4) demonstrate the results of your experiments and project.
  4. Students are strongly encouraged to watch the two video tapes (see the instructor) related to the topics covered in this course.
  5. The Instructor welcomes all bright ideas for improving the quality of this course.

7. Tentative Course Contents: 10 Chapters: Read a minimum of one chapter/week.

Chapter 1: Connecting to the New Wave of Microcomputer Instrumentation, 1

1-1 Joining the Microcomputer Age, 1
1-2 Working with Digital Data, 7
1-3 Making the Computer"Intelligent", 14
1-4 Using the Microcomputer in Science and Technology, 18

Chapter 2: Converting and Acquiring Data in Scientific Instrumentation, 23

2-1 Sensing Digitally, 23
2-2 A Closer Look at Analog Data Encoding, 28
2-3 Converting between Analog and Digital Encoding, 34
2-4 Measuring Time, 39
2-5 Using the Laboratory Interfaced Microcomputer, 46

Chapter 3: Understanding and Measuring Analog Signals, 57

3-1 Starting with the Basics, 58
3-2 Measuring Analog Electrical Quantities, 62
3-3 Assessing Errors in Analog Data Measurement and Transfer, 69
3-4 Using the Oscilloscope To Observe Signals, 72

Chapter 4: Supplying Power to Instruments and Computers, 85

4-1 Characterizing Power Supplies, 85
4-2 Supplying Power with Batteries, 87
4-3 Regulating dc Voltages (dc to dc Conversion), 90
4-4 Converting Voltages from ac to dc, 97
4-5 Isolating and Changing ac Voltages, 103
4-6 Inverting Voltages from dc to ac, 108
4-7 Protecting Instruments and Their Power Supplies, 110
4-8 Regulating dc Current, 117
4-9 Converting Light into Electrical Power, 118

Chapter 5: Manipulating Analog Data with Operational Amplifiers and Servo Systems, 121

5-1 Controlling and Measuring Analog Quantities, 121
5-2 Comparing Analog Signal Levels by Using Operational Amplifiers, 125
5-3 Creating Ideal Voltage Sources, 130
5-4 Processing Analog Signals with Operational Amplifier Current Followers, 133
5-5 Adding and Subtracting Currents and Voltages, 141
5-6 Integrating and Differentiating Analog Signals, 144

Chapter 6: Thinking Digital: Logic Gates, Flip Flops, and Counters, 151

6-1 Implementing Basic Logic with Digital Gates, 151
6-2 Comparing Digital Data, 161
6-3 Selecting/Multiplexing Digital Data, 165
6-4 Decoding Binary Data, 166
6-5 Connecting Gates to the Computer Bus,171
6-6 Storing Digital Data in Flip Flops, 175
6-7 Encoding and Storing Digital Data in Registers, 180
6-8 Shifting Digital Data in Registers, 185
6-9 Connecting Input/Output (I/O) Devices to the CPU Bus, 187
6-10 Measuring Analog Data by Digitization and Counting, 188

Chapter 7: Generating, Switching, and Processing Analog Signals, 191

7-1 Generating Waveforms, 191
7-2 Amplifying Analog Signals with Operational Amplifier Circuits, 200
7-3 Limiting Bandwidth with Active Filters, 219
7-4 Examining Nonideality of Operational Amplifier Circuits, 228
7-5 Digital to Analog Conversion, 235

Chapter 8: Sensing and Controlling in Automation and Robotics, 241

8-1 Controlling Physical and Chemical Quantities, 241
8-2 Transducer Principles, 243
8-3 Energy Conversion Transducers, 246
8-4 Resistive, Capacitive, and Inductive Transducers, 255
8-5 Limiting Current Transducers, 262
8-6 Output Transducers, 267
8-7 Automatic Control Systems, 282
8-8 Laboratory Robotics, 293

Chapter 9: Getting the Most from Real World Signals, 299

9-1 Optimizing Data Acquisition, 299
9-2 Enhancing Signal to Noise Ratio by Bandwidth Reduction, 309
9-3 Enhancing Signal to Noise Ratio by Correlation Techniques, 317
9-4 Measuring the Rate of Events, 325

Chapter 10: Troubleshooting Your Instruments, 329

10-1 Understanding the Process, 329
10-2 Following the Data Flow, 333
10-3 Fixing it Yourself, 338
10-4 Making the Right Connections, 349

Highly-Recommended Additional Reading

Read Supplement 1: Generating and Controlling Analog Electrical Quantities, 351

S1-1 Electrical Quantities, 351
S1-2 Series dc Circuits, 357
S1-3 Ground and Circuit Common, 360

Read Supplement 2: Describing Waveforms and Reactive Circuits, 363

S2-1 Sine Wave Signals, 363
S2-2 ac Signals, 364
S2-3 Measures of Periodic Signal Amplitude, 367
S2-4 Reactive Circuits, 369

Read Supplement 3: Understanding Diodes, Transistors, and Other Solid State Devices, 381

S3-1 Bipolar Devices, 381
S3-2 Field Effect Transistor (FET) Devices, 386
S3-3 Analog Switches, 389
S3-4 Power Control Switches, 391
S3-5 Transistor Amplifiers, 394
S3-6 The Operational Amplifier (OP Amp), 399

Read Appendix A: Grounding and Shielding, 401

A-1 Grounding, 401
A-2 Shielding, 405
A-3 Isolation, 407
A-4 Radio Frequency (RF) Shielding, 408
A-5 Guarding, 408

Read Appendix B: Components, 411

B-1 Resistors, 411
B-2 Conductors, 419
B-3 Capacitors, 422
B-4 Inductors and Transformers, 430

Read Appendix C: Digital Data Transmission, 433

C-1 Transmission Lines, 433
C-2 Line Drivers and Receivers, 435
C-3 Serial Communication Standards, 436

8. TENTATIVE LIST OF 12 EXPERIMENTS:

Conduct and re-conduct a minimum of one experiment/week.

SECTION A DIGITAL MEASUREMENT, 1
Encoding, decoding and displaying information.

A-1 Thermistor Temperature measurement with Digital Multimeter
A-2 Light Measurement with a Photodiode
A-3 Continuity Testing of a Breadboard with the Digital Ohmmeter

SECTION B ELECTRICAL RESISTANCE, CURRENT, VOLTAGE, AND CHARGE, 7
Understanding and measuring analog quantities.

B-1 Resistor Identification and Measurement
B-2 Series Circuits
B-3 Voltage Sources and Loading
B-4 Current measurements and Sources
B-5 Thermistor with constant Current Source

SECTION C REGULATED POWER SUPPLIES, 19
Supplying power for instruments.

C-1 Breadboarding the +5 V and 5 V Regulators
C-2 Testing the Regulators
C-3 Permanent Mounting of Regulators

SECTION D COMPARATORS AND VOLTAGE FOLLOWERS, 24
Using Op Amps as servo comparator and voltage followers.

D-1 The Voltage Comparator
D-2 Voltage Follower
D-3 Follower with Gain

SECTION E CURRENT FOLLOWER AND SUMMING AMPLIFIER, 30
Transforming and processing analog data with OP Amps.

E-1 Current Follower
E-2 Current Summing
E-3 Op Amp Inverting Amplifier
E-4 Voltage Summing Amplifier

SECTION F DIGITAL LOGIC GATES, 36
Thinking digital with logic gates and truth tables.

F-1 Connection of Logic Gates and Indicator Circuits
F-2 The AND Logic Gate and TTL Logic Levels
F-3 The OR Gate
F-4 NAND Gate
F-5 Exclusive OR Gate
F-6 Equality Gate and Inverter

SECTION G FLIP FLOP AND REGISTERS, 42
Storing and shifting digital data in flip-flops.

G-1 Connection of IC's and Completion of Logic level Indicator
G-2 Flip Flops
G-3 Shift Registers

SECTION H SWITCHING, RC CIRCUITS, AND MULTIVIBRATORS, 49
Generating and switching electrical signals.

H-1 Timing in RC Circuits
H-2 Sample and Hold
H-3 An RC Time Delay Circuit
H-4 RC Oscillator

SECTION I DECADE COUNTER, 56
Measuring using electronic counting.

I-1 Up/Down Counting
I-2 Counter Gate and Preset

SECTION J DIGITAL TO ANALOG AND ANALOG TO DIGITAL CONVERTERS, 61
Converting data from digital-to-analog and analog-to-digital.

J-1 Digital to analog converter
J-2 Analog to digital converter

SECTION K FAMILIARIZATION WITH THE OSCILLOSCOPE, 65

Experiments under this section must be conducted by all students

SECTION L INDEPENDENT PROJECT IN COMPUTER INTERFACING AND PROGRAMMING

L 1 Selection of Project

Note: You must finalize this selection (in consultation with the course instructor) one week after the midterm exam.

L 2 Project Report and Demonstration

Note: You must hand in a typed written report one week after the end of classes. Projects should be demonstrated before the final exams.

OTHER IMPORTANT NOTES: To perform these experiments you will need the following:

  1. Experimenter's Kit, located in Cor 406.
  2. 3 1/2 digit digital multimeter.
  3. Screwdriver.
  4. Needlenose pliers.
  5. Function generator.
  6. Oscilloscope.

ADDITIONAL READING

Supplement 1: Controlling and Measuring with Servo Systems, 83
Supplement 2: Troubleshooting Electronic Instrumentation, 85 

© 2007 Montaser Research Group. The George Washington Univeristy.